Microscale deformation behavior of bicrystal boundaries in pure tin (Sn) using micropillar compression
<Abstrate>
Uniaxial compression experiments on micron-sized bicrystalline and single-crystalline
pillars in tin (Sn) using a flat punch nanoindenter tip, have enabled us to quantify the
difference in stress-strain behavior associated with grain boundaries in tin. It was
found that bicrystalline micropillars containing a twin boundary nearly parallel to the
loading axis were characterized by numerous strain bursts and a yield stress either
lower than or comparable to its single-crystalline counterparts. Transmission electron
microscopy on the deformed micropillar revealed that the twin boundary migration
is associated with partial dislocation activity. The slip systems interacting with the
boundary have also been identified using stereographic projections. Micropillar
compression indicated different findings for bicrystalline pillars containing random
angle grain boundaries, which displayed strengthening by acting as a barrier to
dislocation glide. These results indicate that the grain boundary character plays a
very crucial role in controlling the mechanical response of Sn-rich solder joints
and provide insights into the deformations mechanisms occurring at different boundaries.
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